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24448-94-0

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Basic Information
CAS No.: 24448-94-0
Name: 5,5-DIMETHYLBARBITURIC ACID
Article Data: 21
Molecular Structure:
Molecular Structure of 24448-94-0 (5,5-DIMETHYLBARBITURIC ACID)
Formula: C6H8 N2 O3
Molecular Weight: 156.141
Synonyms: Barbituricacid, 5,5-dimethyl- (6CI,7CI,8CI); 5,5-Dimethyl barbituric acid; NSC 120194
Density: 1.235g/cm3
Melting Point: 278-279oC
Boiling Point: °Cat760mmHg
Flash Point: °C
Solubility: 2.829g/L(25 oC)
PSA: 75.27000
LogP: 0.03620
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Synthetic route
1619-62-1

2,2-dimethylmalonic acid diethyl ester

57-13-6

urea

24448-94-0

5,5-dimethylbarbituric acid

Conditions
ConditionsYield
Stage #1: 2,2-dimethylmalonic acid diethyl ester With sodium ethanolate In ethanol at 20℃; for 1h;
Stage #2: urea In ethanol for 15h; Time; Reflux;		81.48%
With sodium ethanolate In ethanol at 80℃; for 16h; Inert atmosphere;36.5 g
77-78-1

dimethyl sulfate

sodium 5-methylbarbiturate

24448-94-0

5,5-dimethylbarbituric acid

Conditions
ConditionsYield
With acetic acid In water at 20℃; for 24h;13%

sodium barbiturate

77-78-1

dimethyl sulfate

24448-94-0

5,5-dimethylbarbituric acid

Conditions
ConditionsYield
With acetic acid In water at 20℃; for 24h;3%
102-09-0

bis(phenyl) carbonate

41882-44-4

2,2-dimethylmalonamide

24448-94-0

5,5-dimethylbarbituric acid

Conditions
ConditionsYield
at 220 - 245℃;

6-amino-5,5-dimethyl-2-thioxo-2,5-dihydro-3H-pyrimidin-4-one

64-19-7

acetic acid

24448-94-0

5,5-dimethylbarbituric acid

Conditions
ConditionsYield
at 150℃; im Rohr;
57-13-6

urea

5659-93-8

2,2-Dimethylmalonyl chloride

24448-94-0

5,5-dimethylbarbituric acid

Conditions
ConditionsYield
at 130℃;
57-13-6

urea

595-46-0

2,2-dimethylmalonic acid

24448-94-0

5,5-dimethylbarbituric acid

Conditions
ConditionsYield
With trichlorophosphate
With sulfuric acid
41882-44-4

2,2-dimethylmalonamide

105-58-8

Diethyl carbonate

24448-94-0

5,5-dimethylbarbituric acid

Conditions
ConditionsYield
With ethanol; sodium ethanolate at 120℃;
67-56-1

methanol

barbituric acid ; silver-salt

74-88-4

methyl iodide

24448-94-0

5,5-dimethylbarbituric acid

...Expand
7647-01-0

hydrogenchloride

2,6-diamino-5,5-dimethyl-5H-pyrimidin-4-one

24448-94-0

5,5-dimethylbarbituric acid

Conditions
ConditionsYield
at 130℃; im Rohr;
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