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2523-44-6

Basic Information
CAS No.: 2523-44-6
Name: 2-Chlorofluorene
Article Data: 30
Molecular Structure:
Molecular Structure of 2523-44-6 (2-Chlorofluorene)
Formula: C13H9 Cl
Molecular Weight: 200.667
Synonyms: Fluorene,2-chloro- (6CI,7CI,8CI); 2-Chlorofluorene; NSC 97412
Density: 1.251 g/cm3
Melting Point: 96-97°C
Boiling Point: 333.4 °C at 760 mmHg
Flash Point: 157.5 °C
Appearance: white crystal
PSA: 0.00000
LogP: 3.91120
Synthetic route

5-chloro-2-phenyl-benzyl chloride

2523-44-6

2-chloro-9H-fluorene

Conditions
ConditionsYield
With bis-triphenylphosphine-palladium(II) chloride; caesium carbonate; Trimethylacetic acid In tetrahydrofuran at 25℃; for 18h; Glovebox; Schlenk technique; Inert atmosphere;99%

[2-(3-chlorobenzyl)phenyl]trimethylsilane

2523-44-6

2-chloro-9H-fluorene

Conditions
ConditionsYield
With [bis(acetoxy)iodo]benzene; (R)-10-camphorsulfonic acid; tetrahydrothiophene gold(III) bromide In methanol; chloroform at 27℃; for 3h; Schlenk technique; Inert atmosphere;90%
179526-95-5

2-bromo-4,4’-dichloro-1,1’-biphenyl

18107-18-1

diazomethyl-trimethyl-silane

2523-44-6

2-chloro-9H-fluorene

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); potassium acetate; potassium carbonate In 1,4-dioxane at 100℃; for 24h; Inert atmosphere;90%
343945-64-2

2-iodo-4’-chlorobiphenyl

74-95-3

1,1-dibromomethane

2523-44-6

2-chloro-9H-fluorene

Conditions
ConditionsYield
With potassium acetate; palladium diacetate; potassium hydrogencarbonate; isopropyl alcohol In N,N-dimethyl acetamide; water; N,N-dimethyl-formamide at 75℃; for 10h; Schlenk technique; Inert atmosphere;84%

(E)-1-((4′-chloro-2′-methyl-[1,1′-biphenyl]-2-yl)diazenyl)-pyrrolidine

2523-44-6

2-chloro-9H-fluorene

Conditions
ConditionsYield
With trifluoroacetic acid In toluene at 100℃; for 1h;75%

2-iodo-4-chlorobiphenyl

74-95-3

1,1-dibromomethane

2523-44-6

2-chloro-9H-fluorene

Conditions
ConditionsYield
With potassium acetate; palladium diacetate; potassium hydrogencarbonate; isopropyl alcohol In N,N-dimethyl acetamide; water; N,N-dimethyl-formamide at 75℃; for 10h; Schlenk technique; Inert atmosphere;64%
7719-09-7

thionyl chloride

86-73-7

9H-fluorene

2523-44-6

2-chloro-9H-fluorene

7791-25-5

sulfuryl dichloride

86-73-7

9H-fluorene

60-29-7

diethyl ether

2523-44-6

2-chloro-9H-fluorene

86-73-7

9H-fluorene

7782-50-5

chlorine

2523-44-6

2-chloro-9H-fluorene

86-73-7

9H-fluorene

67-66-3

chloroform

7782-50-5

chlorine

2523-44-6

2-chloro-9H-fluorene

Conditions
ConditionsYield
at 0 - 5℃;
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Chemistry

Molecular Structure:

Molecular Formula: C13H9Cl
Molecular Weight: 200.6636
IUPAC Name: 2-Chloro-9H-fluorene
Synonyms of 2-Chlorofluorene (CAS NO.2523-44-6): AI3-01713 ; NSC 97412 ; 9H-Fluorene, 2-chloro- (9CI) ; Fluorene, 2-chloro- (8CI)
CAS NO: 2523-44-6
Product Categories: Electronic Chemicals
Melting point: 96-97°C 
Index of Refraction: 1.653
Molar Refractivity: 58.69 cm3
Molar Volume: 160.2 cm3
Surface Tension: 48.3 dyne/cm
Density: 1.251 g/cm3
Flash Point: 157.5 °C
Enthalpy of Vaporization: 55.34 kJ/mol
Boiling Point: 333.4 °C at 760 mmHg
Vapour Pressure of 2-Chlorofluorene (CAS NO.2523-44-6): 0.000265 mmHg at 25°C