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Basic Information
| CAS No.: | 88192-20-5 |
|---|---|
| Name: | 1-Butamine 4-azide |
| Article Data: | 24 |
| Molecular Structure: | |
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| Formula: | C4H10N4 |
| Molecular Weight: | 114.15 |
| Synonyms: | 1-Butanamine,4-azido;4-Azido-1-butanamine;1-amino-4-azidobutane;4-azido-1-butylamine;6-azidobutylamine;4-azido-butylamine;1-azido-4-aminobutane; |
| Density: | g/cm3 |
| Boiling Point: | °Cat760mmHg |
| Flash Point: | °C |
| PSA: | 75.77000 |
| LogP: | 1.18866 |
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Synthetic route
- 24345-72-0
1,4-diazidobutane
- 88192-20-5
4-azidobutan-1-amine
Conditions
| Conditions | Yield |
|---|---|
| With hydrogenchloride; triphenylphosphine In diethyl ether; water; ethyl acetate at 20℃; for 24h; | 88% |
| With hydrogenchloride; water; triphenylphosphine In diethyl ether; ethyl acetate at 0 - 20℃; for 25h; | 88% |
| With hydrogenchloride; triphenylphosphine In diethyl ether; water; ethyl acetate at 0 - 20℃; for 25h; Inert atmosphere; | 88% |
- 177489-76-8
1-azido-4-isocyanatobutane
- 88192-20-5
4-azidobutan-1-amine
Conditions
| Conditions | Yield |
|---|---|
| With sodium hydroxide In tetrahydrofuran for 4h; Heating; | 83% |
- 66917-06-4
N-(4-azidobutyl)phthalimide
- 88192-20-5
4-azidobutan-1-amine
Conditions
| Conditions | Yield |
|---|---|
| With hydrazine hydrate In ethanol for 24h; | 62% |
| With hydrazine hydrate In tetrahydrofuran at 60℃; for 4h; | |
| With hydrazine In methanol Inert atmosphere; |
- 110-60-1
1,4-diaminobutane
- 88192-20-5
4-azidobutan-1-amine
Conditions
| Conditions | Yield |
|---|---|
| With triflic azide; potassium carbonate; copper(II) sulfate In methanol; water | 61% |
- 88192-20-5
4-azidobutan-1-amine
Conditions
| Conditions | Yield |
|---|---|
| With sodium azide In water at 80℃; for 15h; | 50% |
Conditions
| Conditions | Yield |
|---|---|
| With triflic azide; potassium carbonate; copper(II) sulfate In water for 18h; Inert atmosphere; | A 30% B 40% |
- 129392-85-4
N-t-butoxycarbonyl-4-azidobutylamine
- 88192-20-5
4-azidobutan-1-amine
Conditions
| Conditions | Yield |
|---|---|
| With hydrogenchloride In ethyl acetate at 20℃; for 72h; | |
| With trifluoroacetic acid In dichloromethane at 20℃; for 16h; |
- 24345-72-0
1,4-diazidobutane
- 603-35-0
triphenylphosphine
A
- 88192-20-5
4-azidobutan-1-amine
B
- 791-28-6
Triphenylphosphine oxide
Conditions
| Conditions | Yield |
|---|---|
| With hydrogenchloride; water In diethyl ether; hexane at 0℃; modified Staudinger reaction; |
...Expand
- 110-52-1
1,4-dibromo-butane
- 88192-20-5
4-azidobutan-1-amine
Conditions
| Conditions | Yield |
|---|---|
| With sodium azide In water; N,N-dimethyl-formamide at 80 - 85℃; for 8h; | 343.7 g |
| Stage #1: 1,4-dibromo-butane With sodium azide In water; N,N-dimethyl-formamide at 80 - 90℃; for 12h; Stage #2: With hydrogenchloride; triphenylphosphine In water at 25 - 35℃; for 12h; |
- 33977-38-7
1-bromo-4-aminobutane
- 88192-20-5
4-azidobutan-1-amine
Conditions
| Conditions | Yield |
|---|---|
| With sodium azide In water at 80℃; | 620 mg |
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1-Butamine 4-azide
