8-benzoyloxy-3-methyl-isocoumarin

Base Information

• Chemical Name: 8-benzoyloxy-3-methyl-isocoumarin
• CAS No.: 101445-89-0
• Molecular Formula: C₁₇H₁₂O₄
• Molecular Weight: 280.28
• Mol file: 101445-89-0.mol

Synonyms:

Chemical Property of 8-benzoyloxy-3-methyl-isocoumarin

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 8-benzoyloxy-3-methyl-isocoumarin

There total 3 articles about 8-benzoyloxy-3-methyl-isocoumarin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-methoxy-6-((E)-prop-1-enyl)benzoic acid (143112-20-3) → 8-benzoyloxy-3-methyl-isocoumarin (101445-89-0)

Guidance literature:

Multi-step reaction with 2 steps

1: bromine; acetic acid / Erhitzen des Reaktionsprodukts auf 220grad

2: pyridine

With pyridine; bromine; acetic acid;

Reference yield:

3,4-dihydro-8-methoxy-3-methylisocoumarin (30407-92-2) → 8-benzoyloxy-3-methyl-isocoumarin (101445-89-0)

Guidance literature:

Multi-step reaction with 3 steps

1: KOH

2: bromine; acetic acid / Erhitzen des Reaktionsprodukts auf 220grad

3: pyridine

With pyridine; potassium hydroxide; bromine; acetic acid;

Reference yield:

8-hydroxy-3-methyl-1H-isochromene-1-one (1642-85-9) + benzoyl chloride (98-88-4) → 8-benzoyloxy-3-methyl-isocoumarin (101445-89-0)

Guidance literature:

With pyridine;

upstream raw materials:

8-hydroxy-3-methyl-1H-isochromene-1-one

benzoyl chloride

2-methoxy-6-((E)-prop-1-enyl)benzoic acid

3,4-dihydro-8-methoxy-3-methylisocoumarin