10-hydroxydecyl Acetate

Base Information

• Chemical Name: 10-hydroxydecyl Acetate
• CAS No.: 59694-62-1
• Molecular Formula: C12H24O3
• Molecular Weight: 216.321
• Nikkaji Number: J766.851A
• Mol file: 59694-62-1.mol

Synonyms:10-hydroxydecyl Acetate;1,10-decanediol monoacetate;SCHEMBL6060438;ISPBFHJVEYJABG-UHFFFAOYSA-N

Chemical Property of 10-hydroxydecyl Acetate

Chemical Property:

• XLogP3: 2.9
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 11
• Exact Mass: 216.17254462
• Heavy Atom Count: 15
• Complexity: 146

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=O)OCCCCCCCCCCO

Technology Process of 10-hydroxydecyl Acetate

There total 3 articles about 10-hydroxydecyl Acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

methanol (67-56-1) + acetic acid 10-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-decyl ester → 10-acetoxydecane-1-ol (59694-62-1) + bis(4-methoxyphenyl)phenylmethyl methyl ether (125016-87-7)

Guidance literature:

With lithium tetrafluoroborate; In dichloromethane; at 20 ℃; for 0.25h;

DOI:10.1080/00397919908085970

Reference yield:

1,10-Decanediol (112-47-0) + acetic acid (64-19-7,77671-22-8) → 1,10-decanediol diacetate (26118-61-6) + 10-acetoxydecane-1-ol (59694-62-1)

Guidance literature:

sulfuric acid; In water; toluene; for 3h; Heating / reflux;

Reference yield:

1,10-Decanediol (112-47-0) + acetyl chloride (75-36-5) → 1,10-decanediol diacetate (26118-61-6) + 10-acetoxydecane-1-ol (59694-62-1)

Guidance literature:

With silica gel; for 2h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Ambient temperature;

DOI:10.1039/a707753j

upstream raw materials:

1,10-Decanediol

acetyl chloride

methanol

acetic acid

Downstream raw materials:

1,10-decanedioic acid

1-acetoxy-10-(benzyloxy)decane

n-decyl acetate

1,10-Decanediol

Refernces

• 1、 Chen, Anqi,Zheng, Yong,Zhou, Xinfeng. "Lithium tetrafluoroborate: A mild and efficient reagent for the cleavage of dimethoxytrityl ethers". . p. 3421 - 3423. Retrieved 2007/10/03.