N-Methyldidecylamine

Base Information

• Chemical Name: N-Methyldidecylamine
• CAS No.: 7396-58-9
• Molecular Formula: C21H45N
• Molecular Weight: 311.595
• Hs Code.: 2921199090
• European Community (EC) Number: 230-990-1
• UN Number: 2735
• DSSTox Substance ID: DTXSID5027649
• Nikkaji Number: J278.807A
• Wikidata: Q72490061
• Mol file: 7396-58-9.mol

Synonyms:N-Methyldidecylamine;Didecylmethylamine;7396-58-9;N-decyl-N-methyldecan-1-amine;1-Decanamine, N-decyl-N-methyl-;methyldidecylamine;didecyl methylamine;Di(decyl)methylamine;Radiamine 6310;Didecylamine, N-methyl-;Dama 1010;Didecyl methyl amine;EINECS 230-990-1;EC 230-990-1;N,N-didecylmethylamine;DAMA-10;Didecilmetilamina;Metildidecilamina;di-n-decylmethylamine;Amine M210D;Armeen M 210D;Armeen M2-10D;Didecilamina, N-metil-;N N-Didecyl-N-methylamine;N-Methyldidecylamine, 95%;Methyl decyl-1-amino decane;SCHEMBL313415;DTXSID5027649;1-decanamina, n-decil-n-metil-;Methylamine, N,N-bis(N-decyl)-;MFCD00077727;Didecylamine N-methyl-(6CI7CI8CI);AKOS015914849;2,3,4,5,6-pentachlorophenol;quinoline;D2311;FT-0625178;F71200;A837983

Chemical Property of N-Methyldidecylamine

Chemical Property:

• Appearance/Colour: clear slightly light yellow liquid with a fishlike odor
• Vapor Pressure: 1.6E-05mmHg at 25°C
• Melting Point: -7.4 °C
• Refractive Index: n20/D 1.448
• Boiling Point: 365.2 °C at 760 mmHg
• PKA: 9.83±0.50(Predicted)
• Flash Point: 165.1 °C
• PSA: 3.24000
• Density: 0.814 g/cm³
• LogP: 7.19960
• Water Solubility.: 1.2μg/L
• XLogP3: 9.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 18
• Exact Mass: 311.355200440
• Heavy Atom Count: 22
• Complexity: 170
• Transport DOT Label: Corrosive

Purity/Quality:

98% ^*data from raw suppliers

N-?Methyldidecylamine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCCCCCCCN(C)CCCCCCCCCC
• Uses: N-?Methyldidecylamine is a reagent used in the synthesis of novel anthraquinone compounds which act as potential anticancer compounds.

Technology Process of N-Methyldidecylamine

There total 12 articles about N-Methyldidecylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.7%

1-Decanol (112-30-1) + methylamine (74-89-5) → N-methyldidecylamine (7396-58-9)

Guidance literature:

With hydrogen; at 195 ℃; for 4.1h; under 772.577 - 1200.12 Torr;

Reference yield: 76.0%

N-methyldecanoic acid amide (23220-25-9) → N-methyldecan-1-amine (7516-82-7) + N-methyldidecylamine (7396-58-9)

Guidance literature:

With α-Me3Si-γ-Me3SiO-poly[oxy(methylsilanediyl)]; (μ₃,η²,η³,η⁵-acenaphthylene)Ru(CO)7; In various solvent(s); at 40 ℃; for 24h;

DOI:10.1021/jo070591c

Reference yield: 48.0%

methanol (67-56-1) + didecylamine (1120-49-6) → N-methyldidecylamine (7396-58-9)

Guidance literature:

With rhodium(III) chloride hydrate; potassium tert-butylate; at 150 ℃; for 48h; Sealed tube; High pressure;

DOI:10.1002/cctc.202001937

upstream raw materials:

formaldehyd

formic acid

didecylamine

N-methyldecanoic acid amide

Downstream raw materials:

didecyldimethylammonium chloride

Refernces

• 1、 Sarki, Naina,Goyal, Vishakha,Tyagi, Nitin Kumar,Puttaswamy,Narani, Anand,Ray, Anjan,Natte, Kishore. "Simple RuCl3-catalyzed N-Methylation of Amines and Transfer Hydrogenation of Nitroarenes using Methanol". . p. 1722 - 1729. Retrieved 2021/04/19.
• 2、 Goyal, Vishakha,Gahtori, Jyoti,Narani, Anand,Gupta, Piyush,Bordoloi, Ankur,Natte, Kishore. "Commercial Pd/C-Catalyzed N-Methylation of Nitroarenes and Amines Using Methanol as Both C1 and H2 Source". . p. 15389 - 15398. Retrieved 2019/12/04.