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Basic Information
| CAS No.: | 883267-70-7 |
|---|---|
| Name: | 2-(2,4,5-TRIFLUOROPHENYL)-ETHANOL |
| Article Data: | 6 |
| Molecular Structure: | |
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| Formula: | C8H7 F3 O |
| Molecular Weight: | 176.138 |
| Synonyms: | 2-(2,4,5-Trifluorophenyl)ethan;2-(2,4,5-Trifluorophenyl)ethanol, JRD, 97% |
| Density: | 1.33g/cm3 |
| Boiling Point: | 205.3°C at 760 mmHg |
| Flash Point: | 88.8°C |
| PSA: | 20.23000 |
| LogP: | 1.63870 |
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Synthetic route
- 209995-38-0
(2,4,5-trifluorophenyl)acetic acid
- 883267-70-7
2-(2,4,5-trifluorophenyl)ethanol
Conditions
| Conditions | Yield |
|---|---|
| With sodium tetrahydroborate; methanesulfonic acid In tetrahydrofuran at -15 - 10℃; | 98% |
| With dimethylsulfide borane complex In diethyl ether; water at 0 - 20℃; for 1h; | 93.9% |
| Stage #1: (2,4,5-trifluorophenyl)acetic acid With lithium aluminium tetrahydride In tetrahydrofuran at 0 - 20℃; for 6h; Stage #2: With water; sodium hydroxide for 18.3333h; | 92% |
| Stage #1: (2,4,5-trifluorophenyl)acetic acid With sulfuric acid In methanol for 3h; Heating; Stage #2: With diisobutylaluminium hydride In tetrahydrofuran; toluene at 20℃; Reagent/catalyst; Temperature; Solvent; Cooling with ice; | 90% |
- 1036273-20-7
2,4,5-trifluorophenylacetic acid methyl ester
- 883267-70-7
2-(2,4,5-trifluorophenyl)ethanol
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: 2,4,5-trifluorophenylacetic acid methyl ester With sodium tetrahydroborate In tetrahydrofuran at 65℃; for 0.25h; Stage #2: With methanol In tetrahydrofuran for 2.5h; Reflux; | 86% |
- 367-23-7
1,2,4-trifluorobenzene
- 883267-70-7
2-(2,4,5-trifluorophenyl)ethanol
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: aluminum (III) chloride / 6 h / Reflux 2: water; sodium hydroxide / 6 h / 30 °C View Scheme | |
| Multi-step reaction with 2 steps 1: aluminum (III) chloride / 8 h / Reflux 2: water; sodium hydroxide / 3.5 h / 0 °C View Scheme |
- 883267-70-7
2-(2,4,5-trifluorophenyl)ethanol
Conditions
| Conditions | Yield |
|---|---|
| With water; sodium hydroxide at 30℃; for 6h; |
- 883267-70-7
2-(2,4,5-trifluorophenyl)ethanol
Conditions
| Conditions | Yield |
|---|---|
| With water; sodium hydroxide at 0℃; for 3.5h; |
- 883267-70-7
2-(2,4,5-trifluorophenyl)ethanol
- 111991-20-9
2-(2,4,5-trifluorophenyl)acetaldehyde
Conditions
| Conditions | Yield |
|---|---|
| With sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; potassium bromide In dichloromethane; water at 0℃; for 1h; | 94% |
| With manganese(IV) oxide In toluene for 8h; Reagent/catalyst; Solvent; Reflux; | 75% |
Conditions
| Conditions | Yield |
|---|---|
| With magnesium sulfate; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In dichloromethane at -20 - 20℃; for 24h; | 93% |
- 883267-70-7
2-(2,4,5-trifluorophenyl)ethanol
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: 2-(2,4,5-trifluorophenyl)ethanol; (S)-ethyl 2-(tert-butoxy)-2-(4-(4,4-dimethylpiperidin-1-yl)-5-(4-hydroxyphenyl)-2,6-dimethylpyridin-3-yl)acetate With di-isopropyl azodicarboxylate In tetrahydrofuran at 20℃; for 18h; Stage #2: With methanol; sodium hydroxide at 75℃; for 16h; | 79% |
- 883267-70-7
2-(2,4,5-trifluorophenyl)ethanol
- 209995-38-0
(2,4,5-trifluorophenyl)acetic acid
Conditions
| Conditions | Yield |
|---|---|
| With manganese(IV) oxide In chloroform for 7h; Reagent/catalyst; Reflux; | 79% |
- 883267-70-7
2-(2,4,5-trifluorophenyl)ethanol
- 134019-73-1
tert-butyl [2-(chlorosulfonyl)ethyl]carbamate
- 1476070-53-7
C15H20F3NO5S
Conditions
| Conditions | Yield |
|---|---|
| With triethylamine In dichloromethane at 0 - 20℃; for 2h; | 78% |
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2-(2,4,5-TRIFLUOROPHENYL)-ETHANOL
