1,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12-Pentacosafluoro-14-iodotetradecane

Base Information

• Chemical Name: 1,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12-Pentacosafluoro-14-iodotetradecane
• CAS No.: 30046-31-2
• Molecular Formula: C14H4 F25 I
• Molecular Weight: 774.05
• Hs Code.: 2903798000
• European Community (EC) Number: 250-014-8
• UNII: F0Y1907HS3
• DSSTox Substance ID: DTXSID2067535
• Nikkaji Number: J28.295B
• Wikidata: Q81985331
• Mol file: 30046-31-2.mol

Synonyms:30046-31-2;1-Iodo-1H,1H,2H,2H-perfluorotetradecane;146983-96-2;1,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12-Pentacosafluoro-14-iodotetradecane;1H,1H,2H,2H-Perfluorotetradecyl iodide;Perfluorolaurylethyl iodide;Tetradecane, 1,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12-pentacosafluoro-14-iodo-;1,1,2,2-Tetrahydroperfluorotetradecyl iodide;F0Y1907HS3;EINECS 250-014-8;1H,1H,2H,2H-Perfluorotetradecyliodide;Tetradecane,1,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12-pentacosafluoro-14-iodo-;2-(Perfluorododec-1-yl)ethyl iodide;UNII-F0Y1907HS3;2-Perfluorododecyl ethyl iodide;SCHEMBL3777011;DTXSID2067535;C14H4F25I;C14 Gamma-Omega Perfluoro Iodine;12:2 FTI;C14-H4-F25-I;MFCD00039413;AKOS015914809;FT-0638903;1-Iodo-1H,1H,2H,2H-perfluorotetradecane 90%;1,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12-Pentacosafluoro-14-iodotetradecane #;1-Iodo-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,13,13,14,14,14-pentacosafluorotetradecane

Chemical Property of 1,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12-Pentacosafluoro-14-iodotetradecane

Chemical Property:

• Boiling Point: 291.3°Cat760mmHg
• Flash Point: 138.7°C
• PSA: 0.00000
• Density: 1.864g/cm³
• LogP: 9.36210
• XLogP3: 10.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 25
• Rotatable Bond Count: 12
• Exact Mass: 773.89585
• Heavy Atom Count: 40
• Complexity: 909

Purity/Quality:

98% ^*data from raw suppliers

1-Iodo-1H,1H,2H,2H-perfluorotetradecane 90% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C(CI)C(C(C(C(C(C(C(C(C(C(C(C(F)(F)F)(F)F)(F)F)(F)F)(F)F)(F)F)(F)F)(F)F)(F)F)(F)F)(F)F)(F)F

Technology Process of 1,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12-Pentacosafluoro-14-iodotetradecane

There total 2 articles about 1,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12-Pentacosafluoro-14-iodotetradecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-iodoheptadecafluorooctane (507-63-1) + 1-iodoperfluorododecane (307-60-8) + ethene (74-85-1) + n-perfluorohexyl iodide (355-43-1) + 1-Iodo-perfluorodecane (423-62-1) → 1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluoro-8-iodooctane (2043-57-4,71215-70-8) + 2-(n-perfluorooctyl)ethyl iodide (2043-53-0,71215-70-8) + 1-iodo-1H,1H,2H,2H-perfluorododecane (2043-54-1,71215-70-8) + 1-iodo-1H,1H,2H,2H-perfluorotetradecane (30046-31-2)

Guidance literature:

Reference yield:

→ 1-iodo-1H,1H,2H,2H-perfluorohexadecane (65510-55-6) + 1-iodo-1H,1H,2H,2H-perfluorooctadecane + 3,3,4,4,5,5,6,6,6-nonafluorohexyliodide (2043-55-2,71215-70-8) + 1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluoro-8-iodooctane (2043-57-4,71215-70-8) + 2-(n-perfluorooctyl)ethyl iodide (2043-53-0,71215-70-8) + 1-iodo-1H,1H,2H,2H-perfluorododecane (2043-54-1,71215-70-8) + 1-iodo-1H,1H,2H,2H-perfluorotetradecane (30046-31-2)

Guidance literature:

Purification / work up;

Reference yield:

1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluoro-8-iodooctane (2043-57-4,71215-70-8) + 2-(n-perfluorooctyl)ethyl iodide (2043-53-0,71215-70-8) + 1-iodo-1H,1H,2H,2H-perfluorododecane (2043-54-1,71215-70-8) + 1-iodo-1H,1H,2H,2H-perfluorotetradecane (30046-31-2) + potassium acrylate (10192-85-5) → 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,13,13,14,14,14-pentacosafluoro-tetradecyl acrylate (34395-24-9) + 1H,1H,2H-perfluoro-1-tetradecene + 1H,1H,2H,2H-tridecafluoro-n-octanol (647-42-7) + 2-(perfluorodecyl)ethanol (865-86-1) + 3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooct-1-ene (25291-17-2) + 1H,1H,2H-perfluorodecene (21652-58-4) + 1H,1H,2H,2H-perfluorobutadecan-1-ol (39239-77-5) + 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-1-decanol (678-39-7) + 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-henicosafluorododec-1-ene (30389-25-4) + 1H,1H,2H,2H-heptadecafluorodecyl acrylate (27905-45-9) + 3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl 2-propenoate (17527-29-6) + 1,1,2,2-Tetrahydroperfluorododecyl acrylate (17741-60-5)

Guidance literature:

With 4-methoxy-phenol; hydroquinone; In tert-butyl alcohol; at 180 - 190 ℃; for 6h; Product distribution / selectivity;

upstream raw materials:

1-iodoheptadecafluorooctane

1-iodoperfluorododecane

ethene

n-perfluorohexyl iodide

Downstream raw materials:

1H,1H,2H,2H-perfluorohexadecan-1-ol

1H,1H,2H,2H-tridecafluoro-n-octanol

2-(perfluorodecyl)ethanol

1H,1H,2H,2H-nonafluoro-1-hexanol

Refernces

• 1、 -. "Purification of fluorinated alcohols". Page/Page column 4. . Retrieved 2008/06/13.